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Beilstein J. Org. Chem. 2018, 14, 2354–2365, doi:10.3762/bjoc.14.211
Graphical Abstract
Scheme 1: Syntheses of gyroscope like platinum and rhodium complexes and dibridgehead diphosphines derived th...
Scheme 2: Synthesis and alkene metathesis of the monophosphorus precursor 1·BH3.
Figure 1: The 13C{1H} NMR spectra (CDCl3, 100 MHz) of in,out-2·2BH3, (in,in/out,out)-2·2BH3, 6·2BH3, and the ...
Scheme 3: Synthesis of the diphosphorus precursor 11·2BH3.
Scheme 4: Truncated approaches to the diphosphorus precursor 11·2BH3 from 10.
Scheme 5: Alkene metathesis of the diphosphorus precursor 11·2BH3.
Scheme 6: Schematic comparison of the key alkene metathesis steps in Scheme 2 and Scheme 5.
Scheme 7: Steps that set the in,in/out,out vs in,out stereochemistry of 2·2BH3 in Scheme 2 and Scheme 5.
Scheme 8: Another non-metal-templated approach to dibridgehead diphosphorus compounds.
Scheme 9: Previously synthesized dibridgehead diphosphine diboranes.
Scheme 10: Alkene metathesis of the tetraalkenyldiphosphine diborane 19·2BH3.